三[4-(5-二氰基亚甲基甲基-2-噻吩基)苯基]胺合成路线 (共 5 条)
反应条件
triethylamine in dichloromethane
T=20°C; 4 h;
参考文献
Leriche, Philippe; Frere, Pierre; Cravino, Antonio; Aleveque, Olivier; Roncali, Jean
Journal of Organic Chemistry, 2007 , vol. 72, # 22 p. 8332 - 8336
反应条件
triethylamine in chloroform
15 h; Heating;
参考文献
Roquet, Sophie; Cravino, Antonio; Leriche, Philippe; Aleveque, Olivier; Frere, Pierre; Roncali, Jean
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3459 - 3466
反应条件
1: 85 percent / Pd(PPh3)4
2: 90 percent / POCl3
3: 76 percent / Et3N
View Scheme
参考文献
Cravino, Antonio; Roquet, Sophie; Leriche, Philippe; Aleveque, Olivier; Frere, Pierre; Roncali, Jean
Chemical Communications, 2006 , # 13 p. 1416 - 1418
反应条件
1: 13 percent / t-BuOK / tetrahydrofuran / 1 h
2: 76 percent / triethylamine / CHCl3 / 15 h / Heating
View Scheme
参考文献
Roquet, Sophie; Cravino, Antonio; Leriche, Philippe; Aleveque, Olivier; Frere, Pierre; Roncali, Jean
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3459 - 3466
反应条件
1: 70 percent / t-BuOK / tetrahydrofuran / 1 h
2: 76 percent / triethylamine / CHCl3 / 15 h / Heating
View Scheme
参考文献
Roquet, Sophie; Cravino, Antonio; Leriche, Philippe; Aleveque, Olivier; Frere, Pierre; Roncali, Jean
Journal of the American Chemical Society, 2006 , vol. 128, # 10 p. 3459 - 3466