4-[4-(二甲基氨基)苯基]-1,2,4-三唑烷-3,5-二酮合成路线 （共 5 条）
反应条件
potassium carbonate in water T=90°C; 3 h;
参考文献
Ogawa, Shoujiro; Ooki, Satoshi; Morohashi, Misato; Yamagata, Kenichiro; Higashi, Tatsuya
Rapid Communications in Mass Spectrometry, 2013 , vol. 27, # 21 p. 2453 - 2460
反应条件
1: sodium azide / acetone; water / 1 h / 0 °C 2: toluene / 0.33 h / |Reflux 3: hydrazinecarboxylic acid ethyl ester / toluene; benzene / 2 h / 20 °C / |Reflux 4: potassium carbonate / water / 3 h / 90 °C View Scheme
参考文献
Rapid Communications in Mass Spectrometry, , vol. 27, # 21 p. 2453 - 2460
反应条件
1: toluene / 0.33 h / |Reflux 2: hydrazinecarboxylic acid ethyl ester / toluene; benzene / 2 h / 20 °C / |Reflux 3: potassium carbonate / water / 3 h / 90 °C View Scheme
参考文献
Rapid Communications in Mass Spectrometry, , vol. 27, # 21 p. 2453 - 2460
反应条件
1: hydrazinecarboxylic acid ethyl ester / toluene; benzene / 2 h / 20 °C / |Reflux 2: potassium carbonate / water / 3 h / 90 °C View Scheme
参考文献
Rapid Communications in Mass Spectrometry, , vol. 27, # 21 p. 2453 - 2460
反应条件
[bis(acetoxy)iodo]benzene in ethyl acetate T=20°C; 3 h;
参考文献
Ogawa, Shoujiro; Ooki, Satoshi; Morohashi, Misato; Yamagata, Kenichiro; Higashi, Tatsuya
Rapid Communications in Mass Spectrometry, 2013 , vol. 27, # 21 p. 2453 - 2460
