1,5-二甲基-1H-吲哚-2-甲醛合成路线 （共 3 条）
反应条件
manganese(IV) oxide in dichloromethane
12 h; Reflux;
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
2: manganese(IV) oxide / dichloromethane / 12 h / Reflux
View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
反应条件
1.1: sulfuric acid / 24 h / Reflux
2.1: sodium hydride / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.2: 0 - 20 °C / Inert atmosphere
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere
4.1: manganese(IV) oxide / dichloromethane / 12 h / Reflux
View Scheme
参考文献
Praveen, Chandrasekaran; Perumal, Paramasivan Thirumalai
Synlett, 2011 , # 4 p. 521 - 524
