(1-乙基-1H-吲哚-3-磺酰基)-乙酸合成路线 （共 3 条）
反应条件
1: With NH2NH2•xH2O; sodium hydroxide in ethanol; water
2 h; HeatingInert atmosphere;
2: With hydrogenchloride in water
T=5°C; pH=1; 12 h;
参考文献
Mirskova; Levkovskaya; Kolesnikova; Perminova; Rudyakova; Adamovich
Russian Chemical Bulletin, 2010 , vol. 59, # 12 p. 2236 - 2246
反应条件
1.1: sodium hydroxide / dimethyl sulfoxide
1.2: 3 h / 10 - 15 °C
2.1: iodine; potassium iodide / ethanol / 3 h / 30 - 40 °C / Inert atmosphere
3.1: NH2NH2•xH2O; sodium hydroxide / ethanol; water / 2 h / Heating; Inert atmosphere
3.2: 12 h / 5 °C / pH 1
View Scheme
参考文献
Mirskova; Levkovskaya; Kolesnikova; Perminova; Rudyakova; Adamovich
Russian Chemical Bulletin, 2010 , vol. 59, # 12 p. 2236 - 2246
反应条件
1.1: iodine; potassium iodide / ethanol / 3 h / 30 - 40 °C / Inert atmosphere
2.1: NH2NH2•xH2O; sodium hydroxide / ethanol; water / 2 h / Heating; Inert atmosphere
2.2: 12 h / 5 °C / pH 1
View Scheme
参考文献
Mirskova; Levkovskaya; Kolesnikova; Perminova; Rudyakova; Adamovich
Russian Chemical Bulletin, 2010 , vol. 59, # 12 p. 2236 - 2246
