potassium cyanide in N,N-dimethyl-formamide
22 h; Ambient temperaturefurther reagent: NaOMe; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
1: With trimethylsilyl iodide in dichloromethane
T=20°C; 24 h;
2: With methanol; cesium fluoride
T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Lukashev, Nikolai V.; Kazantsev, Alexei V.; Borisenko, Anatolii A.; Beletskaya, Irina P.
Tetrahedron, 2001 , vol. 57, # 52 p. 10309 - 10317