2,3-二甲基-2-(三甲基甲硅烷基氧基)丁腈合成路线 （共 4 条）
参考文献
Ohta, Hiromichi; Kimura,Yoichi; Sugano, Yasushi
Tetrahedron Letters, 1988 , vol. 29, # 52 p. 6957 - 6960
反应条件
hydrogenchloride; water
T=85°C; 16 h; optical yield given as percent ee;
参考文献
Caille, Seb; Cui, Sheng; Hwang, Tsang-Lin; Wang, Xiang; Faul, Margaret M.
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3833 - 3842
反应条件
1: iron(III) chloride / 1 h / 0 deg C to room temp.
2: 62 percent / LiN(SiMe3)2 / tetrahydrofuran / -78 °C
View Scheme
参考文献
Hiyama; Oishi; Suetsugu; et al.
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 6 p. 2139 - 2150
反应条件
camphor-10-sulfonic acid; water in 2-methyl tetrahydrofuran
T=23°C; 3 h; Inert atmosphere;
参考文献
Caille, Seb; Cui, Sheng; Hwang, Tsang-Lin; Wang, Xiang; Faul, Margaret M.
Journal of Organic Chemistry, 2009 , vol. 74, # 10 p. 3833 - 3842
