3-(4-甲基-1-哌嗪甲基)苯硼酸频哪酯合成路线 （共 5 条）
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
in tetrahydrofuran T=20°C; 2 h;
参考文献
US2006/84650 A1, ;
Page/Page column 108-109 ;
US 20060084650 A1
反应条件
potassium carbonate in dimethyl sulfoxide T=85°C; 6 h;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 2 p. 196 - 218
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
