3-溴-1,1,1-三氟-2-丙醇合成路线 (共 2 条)
反应条件
baker's yeast in water
T=32°C; 4 h;
参考文献
Bucciarelli, Maria; Forni. Arrigo; Moretti, Irene; Torre, Giovanni
Synthesis, 1983 , # 11 p. 897 - 899
反应条件
(+)-Ipc2BCl; bis-(2-hydroxy-ethyl)-amine
1.) Et2O, -25 deg C, 96 h, 2.) r.t., 2 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Ramachandran, P. Veeraraghavan; Gong, Baoqing; Brown, Herbert C.
Journal of Organic Chemistry, 1995 , vol. 60, # 1 p. 41 - 46