(R)-1-5-甲基 2-((叔丁氧基羰基)氨基)戊二酸苄酯合成路线 (共 3 条)
反应条件
diazomethyl-trimethyl-silane in hexane; dichloromethane
T=0°C; 1 h;
参考文献
MERCK and CO., INC.
Patent: WO2006/44449 A2, 2006 ;
Location in patent: Page/Page column 56 ;
WO 2006/044449 A2
反应条件
in methanol; hexane; dichloromethane
T=0°C;
参考文献
Burgey, Christopher S.; Paone, Daniel V.; Shaw, Anthony W.; Deng, James Z.; Nguyen, Diem N.; Potteiger, Craig M.; Graham, Samuel L.; Vacca, Joseph P.; Williams, Theresa M.
Organic Letters, 2008 , vol. 10, # 15 p. 3235 - 3238
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile
24 h;
参考文献
Burgey, Christopher S.; Paone, Daniel V.; Shaw, Anthony W.; Deng, James Z.; Nguyen, Diem N.; Potteiger, Craig M.; Graham, Samuel L.; Vacca, Joseph P.; Williams, Theresa M.
Organic Letters, 2008 , vol. 10, # 15 p. 3235 - 3238