硫代苯甲酸 S-苯基酯合成路线 (共 180 条)
反应条件
copper acetylacetonate; triphenylphosphine 1.) a) THF, hexane, from -78 deg C to 0 deg C, b) 0 deg C, 10 min, 2.) 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Takai, Kazuhiko; Oshima, Koichiro; Nozaki, Hitosi
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 4 p. 1281 - 1282
反应条件
in cyclohexane T=80°C; 30 h; Irradiation; Product distributionMechanism;
参考文献
Petrova, R. G.; Gasanov, R. G.; Churkina, T. D.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 2 p. 298 - 301
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 2 p. 379 - 382
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; caesium carbonate in N,N-dimethyl-formamide T=95°C; Sonogashira type reaction; 0.75 h; Microwave irradiation;
参考文献
Mehta, Vaibhav Pravinchandra; Sharma, Anuj; Van Der Eycken, Erik
Organic Letters, 2008 , vol. 10, # 6 p. 1147 - 1150
反应条件
triphenylphosphine; nickel dichloride; zinc in N,N-dimethyl-formamide T=80°C; 6 h;
参考文献
Wenkert, Ernest; Chianelli, Donatella
Journal of the Chemical Society, Chemical Communications, 1991 , # 9 p. 627 - 628
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene Heating;
参考文献
Sugoh; Kuniyasu; Sugae; Ohtaka; Takai; Tanaka; Machino; Kambe; Kurosawa
Journal of the American Chemical Society, 2001 , vol. 123, # 21 p. 5108 - 5109
反应条件
isoquinoline T=260°C; 20 h; Further byproducts given. Yields of byproduct given;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; Ismail, Mohamed T.
Canadian Journal of Chemistry, 1982 , vol. 60, p. 2870 - 2875
参考文献
Hauptmann; Wladislaw
Journal of the American Chemical Society, 1950 , vol. 72, p. 707
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Hauptmann; Wladislaw; Camargo
Experientia, 1948 , vol. 4, p. 385
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Hauptmann et al.
Justus Liebigs Annalen der Chemie, 1952 , vol. 576, p. 45,56
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Hauptmann et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 5832
反应条件
isoquinoline T=260°C; 20 h; Mechanism;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; Ismail, Mohamed T.
Canadian Journal of Chemistry, 1982 , vol. 60, p. 2870 - 2875
反应条件
iron (III) acetylacetonate in tetrahydrofuran T=0°C;
参考文献
Cardellicchio, C.; Fiandanese, V.; Marchese, G.; Ronzini, L.
Tetrahedron Letters, 1985 , vol. 26, # 30 p. 3595 - 3598
反应条件
isoquinoline T=260°C; 20 h; Mechanism;
参考文献
Abdel-Wahab, Aboel-Magd A.; El-Khawaga, Ahmed M.; Ismail, Mohamed T.
Canadian Journal of Chemistry, 1982 , vol. 60, p. 2870 - 2875