硫代苯甲酸 S-苯基酯合成路线 （共 180 条）
反应条件
in chloroform
1 h; Ambient temperature;
参考文献
Effenberger, Franz; Bessey, Eberhard
Chemische Berichte, 1980 , vol. 113, # 6 p. 2100 - 2109
反应条件
triphenylphosphine; nickel dichloride; zinc in N,N-dimethyl-formamide
T=50°C; 20 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wenkert, Ernest; Chianelli, Donatella
Journal of the Chemical Society, Chemical Communications, 1991 , # 9 p. 627 - 628
反应条件
in chloroform
0.75 h; Heating;
参考文献
Piepers, Oscar; Kellogg, Richard M.
Journal of the Chemical Society, Chemical Communications, 1980 , # 23 p. 1147 - 1149
反应条件
hydrogen sulfide
T=400°C; Further byproducts given;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Shagun, L. G.; Glukhikh, V. I.; Vitkovskii, V. Yu.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, # 11 p. 2053 - 2056
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 11 p. 2299 - 2302
反应条件
1: 24 percent / BF3*OEt2 / toluene / 0.5 h / -78 °C
2: 1.) lithium naphthalenide / 1.) THF, -78 deg C; 2.) THF, -78 deg C to r.t.
View Scheme
参考文献
Goeppel, Dirk; Muenster, Ingo; Brueckner, Reinhard
Tetrahedron, 1994 , vol. 50, # 12 p. 3687 - 3708
反应条件
in dimethyl sulfoxide
1 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Filiberti, Marcos
Tetrahedron, 1989 , vol. 45, # 23 p. 7411 - 7420
反应条件
tributylphosphine in dichloromethane
参考文献
Grieco,P.A. et al.
Journal of Organic Chemistry, 1978 , vol. <6> 43, p. 1283 - 1285
反应条件
1: 1.) Et3Al / 1.) toluene, 0 deg C then r.t., 1 h; 2.) toluene, 0 deg C, 2 h
2: 1.) lithium naphthalenide / 1.) THF, -78 deg C; 2.) THF, -78 deg C to r.t.
View Scheme
参考文献
Goeppel, Dirk; Muenster, Ingo; Brueckner, Reinhard
Tetrahedron, 1994 , vol. 50, # 12 p. 3687 - 3708
反应条件
1: acetonitrile / 15 min, r.t; 40 min, 40 degC
2: methanesulfonic acid / acetonitrile / 2 h / 60 °C
View Scheme
参考文献
Kitagawa, Tokujiro; Kuroda, Hiroko; Sasaki, Hideaki; Kawasaki, Koichi
Chemical & Pharmaceutical Bulletin, 1987 , vol. 35, # 10 p. 4294 - 4301
反应条件
in tetrahydrofuran
4 h; Ambient temperature;
参考文献
Nagao, Yoshimitsu; Kawabata, Kohji; Seno, Kaoru; Fujita, Eiichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2470 - 2473
