硫代苯甲酸 S-苯基酯合成路线 (共 180 条)
反应条件
1: 80 percent / Et3N / tetrahydrofuran / 9 h / Heating
2: 48 percent / KF/Al2O3 / toluene / 5.5 h / 85 °C
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参考文献
Movassagh, Barahman; Zakinezhad, Yousef
Journal of Chemical Research, 2006 , # 6 p. 369 - 370
反应条件
1: Et3N / petroleum ether
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参考文献
Minich,D. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1969 , p. 795 - 799
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1969 , p. 876 - 880
反应条件
1: COCl2 / toluene
2: (i) Et2O, (ii) H2O
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参考文献
Eilingsfeld,H. et al.
Chemische Berichte, 1963 , vol. 96, p. 2671 - 2690
参考文献
Wheeler; Merriam
Journal of the American Chemical Society, 1901 , vol. 23, p. 298
反应条件
trichlorophosphate
T=120 - 130°C; Erwaermen des Reaktionsprodukts mit Natriumacetat und Wasser;
参考文献
Raison
Journal of the Chemical Society, 1949 , p. 3319,3323
反应条件
T=500°C; P=0.001 - 0.1 Torr; Further byproducts given;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3345 - 3348
反应条件
in diethyl ether
0.5 h;
参考文献
Detty, Michael R.; Wood, Gary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 80 - 89
反应条件
in N,N-dimethyl-formamide
T=70 - 80°C; 1.5 h;
参考文献
You; Chen
Synthesis, 1992 , # 6 p. 521 - 522
反应条件
in diethyl ether
1 h;
参考文献
Detty, Michael R.; Wood, Gary P.
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 80 - 89
反应条件
T=500°C; P=0.001 - 0.1 Torr; Further byproducts given;
参考文献
Aitken, R. Alan; Drysdale, Martin J.; Ryan, Bruce M.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 20 p. 3345 - 3348