硫代苯甲酸 S-苯基酯合成路线 （共 180 条）
反应条件
3,3-dimethyldioxirane in dichloromethane; acetone
T=-30°C;
参考文献
Adam; Hadjiarapoglou
Tetrahedron Letters, 1992 , vol. 33, # 4 p. 469 - 470
反应条件
polystyrene-supported P(1+)(C4H9)3 * Cl(1-) in diethylene glycol dimethyl ether
T=110°C;
参考文献
Nishikubo, Tadatomi; Iizawa, Takashi; Shimojo, Moriyasu; Kato, Tetsuya; Shiina, Atsushi
Journal of Organic Chemistry, 1990 , vol. 55, # 8 p. 2536 - 2542
反应条件
tetrachloromethane; triphenylphosphine
10 h; Heating;
参考文献
Nagashima, Enkou; Suzuki, Kunio; Sekiya, Minoru
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3306 - 3308
反应条件
1: 54 percent / PPh3, CCl4 / 10 h / Heating
2: 83 percent / 1.6M BuLi / pentane; diethyl ether / 1 h / -70 °C
View Scheme
参考文献
Nagashima, Enkou; Suzuki, Kunio; Sekiya, Minoru
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 9 p. 3306 - 3308
反应条件
in ethylene glycol dimethyl ether
T=85°C; 8 h;
参考文献
Yousif, N. M.; Pedersen, U.; Yde, B.; Lawesson, S.-O.
Tetrahedron, 1984 , vol. 40, # 14 p. 2663 - 2670
反应条件
Lawesson's reagent in xylene
T=140°C;
参考文献
Oh, Hyuck Keun; Shin, Chul Ho; Lee, Ikchoon
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1995 , # 6 p. 1169 - 1174
反应条件
in ethylene glycol dimethyl ether
T=80°C; 8 h;
参考文献
Yousif, N. M.; Pedersen, U.; Yde, B.; Lawesson, S.-O.
Tetrahedron, 1984 , vol. 40, # 14 p. 2663 - 2670
反应条件
1: N-chloro-succinimide; ammonium chloride / water; acetonitrile / 0.33 h / 0 °C / pH 0 - 2
2: sodium carbonate / water; acetonitrile / 0.33 h / 0 - 20 °C
View Scheme
参考文献
Ho, Danny K.H.; Chan, Lily; Hooper, Alice; Brennan, Paul E.
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 820 - 823
参考文献
Kumamoto,T. et al.
Bulletin of the Chemical Society of Japan, 1968 , vol. 41, p. 2742 - 2745
反应条件
1: 5-Iodo-pentanoic acid ethyl ester With chloro-trimethyl-silane; ethylene dibromide; zinc in tetrahydrofuran
T=35°C; 20 h;
2: PhSBz With bis(acetylacetonate)nickel(II) in tetrahydrofuran; toluene
T=20°C; 20 h;
参考文献
Shimizu, Toshiaki; Seki, Masahiko
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 1039 - 1042
