硫代苯甲酸 S-苯基酯合成路线 （共 180 条）
反应条件
dipotassium peroxodisulfate; tetraethylammonium bromide in 1,2-dichloro-ethane
T=90°C; 40 h; Inert atmosphere;
参考文献
Zhu, Xuebin; Shi, Yan; Mao, Haibin; Cheng, Yixiang; Zhu, Chengjian
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3558 - 3562
反应条件
N,N-dicyclohexylmethylamine; sodium acetate; palladium diacetate; bis[2-(diphenylphosphino)phenyl] ether; bis(dibenzylideneacetone)-palladium(0); [(t-Bu)3PH]BF4 in ethylene glycol dimethyl ether
T=85°C; 18 h; chemoselective reaction;
参考文献
Burhardt, Mia N.; Taaning, Rolf H.; Skrydstrup, Troels
Organic Letters, 2013 , vol. 15, # 4 p. 948 - 951
反应条件
1: thiophenol With n-butyllithium in tetrahydrofuran; hexane
T=20°C; Metallation; 0.25 h;
2: 1-(2,5-Dichlorophenyl)-2,2-bis(methylsulfanyl)vinyl benzoate in tetrahydrofuran; hexane
Acylation; 1 h; Heating;
参考文献
Degani; Dughera; Fochi; Serra
Synthesis, 1999 , # 7 p. 1200 - 1208
反应条件
triethylamine in dichloromethane
T=25°C; 1 h;
参考文献
Katritzky, Alan R.; Shestopalov, Aleksandr A.; Suzuki, Kazuyuki
Synthesis, 2004 , # 11 p. 1806 - 1813
反应条件
sodium ethanolate in ethanol
T=60°C; 0.5 h;
参考文献
Iwata, Chuzo; Watanabe, Mayumi; Okamoto, Shigeha; Fujimoto, Michitaro; Sakae, Masatoshi; et al.
Heterocycles, 1988 , vol. 27, # 2 p. 323 - 326
反应条件
in chloroform
T=20°C; 2 h;
参考文献
Pan, Xiangcheng; Curran, Dennis P.
Organic Letters, 2014 , vol. 16, # 10 p. 2728 - 2731
反应条件
tetrabutyl-ammonium chloride; sodium hydroxide in dichloromethane; water
T=0°C; 0.0833333 h;
参考文献
Simion, Cristian; Hashimoto, Iwao; Mitoma, Yoshiharu; Simion, Alina Marieta; Egashira, Naoyoshi
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 12 p. 2480 - 2488
反应条件
dicobalt octacarbonyl in benzene
T=275°C; P=733400 Torr;
参考文献
Holmquist,H.E.; Carnahan,J.E.
Journal of Organic Chemistry, 1960 , vol. 25, p. 2240 - 2242
反应条件
hydrogenchloride; N-Nitrosomorpholine; potassium iodide in dichloromethane; water
T=22°C; 44 h;
参考文献
Jorgensen, K. A.; El-Wassimy, M. T. M.; Lawesson, S. -O.
Tetrahedron, 1983 , vol. 39, # 3 p. 469 - 474
反应条件
dicobalt octacarbonyl in benzene
T=180°C; P=56886.3 - 67229.2 Torr; stainless steel autoclave;
参考文献
Antebi, Shlomo; Alper, Howard
Canadian Journal of Chemistry, 1986 , vol. 64, p. 2010 - 2012
