硫代苯甲酸 S-苯基酯合成路线 (共 180 条)
反应条件
copper(l) iodide; 1,10-phenanthroline; N-ethyl-N,N-diisopropylamine in toluene
16 h; Reflux;
参考文献
Ho, Danny K.H.; Chan, Lily; Hooper, Alice; Brennan, Paul E.
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 820 - 823
反应条件
dipotassium peroxodisulfate; tetraethylammonium bromide in 1,2-dichloro-ethane
T=90°C; 40 h; Inert atmosphere;
参考文献
Zhu, Xuebin; Shi, Yan; Mao, Haibin; Cheng, Yixiang; Zhu, Chengjian
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3558 - 3562
反应条件
dicobalt octacarbonyl in benzene
T=300°C; P=760000 Torr;
参考文献
Holmquist,H.E.; Carnahan,J.E.
Journal of Organic Chemistry, 1960 , vol. 25, p. 2240 - 2242
反应条件
water in tert-butyl alcohol
T=125°C; 48 h; Yields of byproduct given;
参考文献
Cox, Christopher; Wack, Harald; Lectka, Thomas
Angewandte Chemie - International Edition, 1999 , vol. 38, # 6 p. 798 - 800
反应条件
aluminium trichloride; zinc in N,N-dimethyl-formamide
T=65°C; 13 h;
参考文献
Movassagh; Lakouraj; Fadaei
Journal of Chemical Research - Part S, 2001 , # 1 p. 22 - 23
反应条件
triethylamine in N,N-dimethyl-formamide
T=70 - 80°C; 6 h;
参考文献
Mashraqui, Sabir H.; Shivaji, Jadhav L.
Journal of Chemical Research - Part S, 2003 , # 3 p. 121 - 123
反应条件
potassium carbonate in ethanol
T=20°C; 4 h;
参考文献
Oku, Akira; Hori-ie, Naofumi; Harada, Toshiro
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 2 p. 609 - 612
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in tetrahydrofuran
T=20°C; arylthiocarbonylation; 7 h;
参考文献
Wang; Chen
Journal of Chemical Research - Part S, 2000 , # 8 p. 372 - 373
反应条件
triethylamine in N,N-dimethyl-formamide
T=75 - 80°C; 4 h;
参考文献
Mashraqui, Sabir Hussain; Shivaji, Jadhav Latika
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 5 p. 927 - 935
反应条件
trifluoroacetic acid
T=0°C;
参考文献
Patra, Pranab K.; Shanmugasundaram, Kandasamy; Matoba, Manabu; Nishide, Kiyoharu; Kajimoto, Tetsuya; Node, Manabu
Synthesis, 2005 , # 3 art. no. F12504SS, p. 447 - 457