1-(N-乙酰基氨基)-2-(4-氯苯基)-乙烷合成路线 (共 5 条)
反应条件
1: H2SO4; AcOH / ethanol / 20 °C 2: HCl / ethanol / Heating View Scheme
参考文献
Bojarski, Andrzej J; Mokrosz, Maria J; Minol, Sijka Charakchieva; Koziol, Aneta; Wesolowska, Anna; Tatarczynska, Ewa; Klodzinska, Aleksandra; Chojnacka-Wojcik, Ewa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 87 - 95
反应条件
triethylamine in dichloromethane
0.5 h; Ambient temperature;
参考文献
Langlois, Michel; Bremont, Beatrice; Shen, Shuren; Poncet, Annie; Andrieux, Jean; et al.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 12 p. 2050 - 2060
反应条件
in toluene
0.75 h; Ambient temperature;
参考文献
Spurr, Paul R.
Tetrahedron Letters, 1995 , vol. 36, # 16 p. 2745 - 2748
反应条件
1: LiAlH4 / diethyl ether / 3 h / Heating
View Scheme
参考文献
Bojarski, Andrzej J; Mokrosz, Maria J; Minol, Sijka Charakchieva; Koziol, Aneta; Wesolowska, Anna; Tatarczynska, Ewa; Klodzinska, Aleksandra; Chojnacka-Wojcik, Ewa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 87 - 95
反应条件
chlorine in tetrachloromethane
T=25°C; Kinetics;
参考文献
O'Connell, Jenny L.; Simpson, Jamie S.; Dumanski, Paul G.; Simpson, Gregory W.; Easton, Christopher J.
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 14 p. 2716 - 2723