1: allyl-magnesium chloride With gallium(III) chloride in tetrahydrofuran; hexane
T=25°C; 0.333333 h;
2: 2-bromo-N,N-dimethylpropionamide With air; triethyl borane in tetrahydrofuran; hexane; water
2 h;
sodium hydrogencarbonate in tetrahydrofuran; water
Ambient temperature; Yield given;
参考文献
Tamaru, Yoshinao; Mizutani, Masato; Furukawa, Yutaka; Kawamura, Shin-ichi; Yoshida, Zen-ichi; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 4 p. 1079 - 1085