2,6-二甲基-4-(3-硝基苯基)-3,5-吡啶二甲酸合成路线 (共 6 条)
反应条件
sodium hydroxide in ethanol
2 h; Heating;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 96 percent / 4N aq. HNO3 / 1 h / Heating
2: 82 percent / NaOH / aq. ethanol / 2 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 80 percent / conc. aq. ammonium hydroxide / methanol / 4 h / Heating
2: 96 percent / 4N aq. HNO3 / 1 h / Heating
3: 82 percent / NaOH / aq. ethanol / 2 h / Heating
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 99 percent / 1.5 h / Heating; heating in Dowterm
2: 100 percent / aq. H2O2, 30percent / acetic acid / 3 h / Heating
3: 0.5 h / Heating
4: conc. HCl / 1 h / Heating
5: 76 percent / activated manganese dioxide / CHCl3 / 6 h / Heating
6: 95 percent / palladium on charcoal / various solvent(s) / 1 h / 190 °C / heating in Dowtherm
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1: 99 percent / 1.5 h / Heating; heating in Dowterm
2: 82 percent / H2 / palladium on charcoal / dimethylformamide
View Scheme
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
反应条件
1.5 h; Heatingheating in Dowterm;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856