lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 25°C; 10.5 h;
参考文献
Fogassy, Katalin; Kovacs, Krisztina; Keseru, Gyoergy M.; Toke, Laszlo; Faigl, Ferenc
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1039 - 1043
1.1: BuLi; TMEDA / diethyl ether / 1 h / 0 °C
1.2: 70 percent / tetrahydrofuran; diethyl ether / 20 °C
2.1: LiAlH4 / tetrahydrofuran / 10.5 h / 0 - 25 °C
View Scheme
参考文献
Fogassy, Katalin; Kovacs, Krisztina; Keseru, Gyoergy M.; Toke, Laszlo; Faigl, Ferenc
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1039 - 1043
1.1: 87 percent / acetic acid
2.1: BuLi; TMEDA / diethyl ether / 1 h / 0 °C
2.2: 70 percent / tetrahydrofuran; diethyl ether / 20 °C
3.1: LiAlH4 / tetrahydrofuran / 10.5 h / 0 - 25 °C
View Scheme
参考文献
Fogassy, Katalin; Kovacs, Krisztina; Keseru, Gyoergy M.; Toke, Laszlo; Faigl, Ferenc
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 9 p. 1039 - 1043
