5-异氰酰基-1-甲基-1H-吲哚合成路线 （共 4 条）
反应条件
1: NaOH / methanol; H2O / 8 h / Heating
2: triethylamine; diphenylphosphorazidate / benzene / 1 h / 20 °C
3: chlorobenzene / 1 h / Heating
View Scheme
参考文献
Rigby, James H.; Burke, Patrick J.
Heterocycles, 2006 , vol. 67, # 2 p. 643 - 653
反应条件
1.1: NaH / dimethylformamide / 1 h / 0 °C
1.2: dimethylformamide / 2.5 h / 0 - 20 °C
2.1: NaOH / methanol; H2O / 8 h / Heating
3.1: triethylamine; diphenylphosphorazidate / benzene / 1 h / 20 °C
4.1: chlorobenzene / 1 h / Heating
View Scheme
参考文献
Rigby, James H.; Burke, Patrick J.
Heterocycles, 2006 , vol. 67, # 2 p. 643 - 653
反应条件
1.1: NaH / dimethylformamide / 1 h / 0 °C
1.2: dimethylformamide / 2.5 h / 0 - 20 °C
2.1: NaOH / ethanol; H2O / 8 h / Heating
3.1: triethylamine; diphenylphosphorazidate / benzene / 1 h / 20 °C
4.1: chlorobenzene / 1 h / Heating
View Scheme
参考文献
Rigby, James H.; Burke, Patrick J.
Heterocycles, 2006 , vol. 67, # 2 p. 643 - 653
反应条件
1: triethylamine; diphenylphosphorazidate / benzene / 1 h / 20 °C
2: chlorobenzene / 1 h / Heating
View Scheme
参考文献
Rigby, James H.; Burke, Patrick J.
Heterocycles, 2006 , vol. 67, # 2 p. 643 - 653
