1-[4-(4,4,5,5-四甲基-1,3,2-二噁硼烷-2-基)苄基]吡咯烷合成路线 （共 4 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=80°C; 1 h;
参考文献
US2011/281842 A1, ;
Page/Page column 75 ;
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; sodium carbonate; bis[2-(diphenylphosphino)phenyl] ether in anhydrous xylene T=155°C; 24 h; Inert atmosphereReflux;
参考文献
Ma, Winson M. J.; James, Tony D.; Williams, Jonathan M. J.
Organic Letters, 2013 , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
反应条件
1: toluene / 2 h / |Dean-Stark; |Reflux; |Inert atmosphere 2: [Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; bis[2-(diphenylphosphino)phenyl] ether; sodium carbonate / anhydrous xylene / 24 h / 155 °C / |Inert atmosphere; |Reflux View Scheme
参考文献
Organic Letters, , vol. 15, # 18 p. 4850 - 4853
