in benzene
byproducts: (C10H4)(C6H5)4; 70°C; 1.5 h;; sublimation in vac.;;
参考文献
Egorov, M. P.; Kolesnikov, S. P.; Struchkov, Yu. T.; Antipin, M. Yu.; Sereda, S. V.; Nefedov, O. M.
Journal of Organometallic Chemistry, 1985 , vol. 290, p. C27 - C30
in benzene-d6
Irradiation (UV/VIS); under Ar; photolysis of digermabicyclooctadiene in C6D6 in the presenceof thiacycloheptyne at room temp. for 5 min; detd. by (1)H CIDNP spectra;