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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88498-80-0
合成路线
（共 10 条）
3722-51-8
西伯尔链接剂
→
反应条件
88498-80-0
反应条件
pyridinium hydrobromide perbromide in acetic acid T=55°C; 0.5 h;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
731-66-8
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 1.2 g / decahydronaphthalene / 3 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
+
106-95-6
3-溴丙烯
→
反应条件
88498-81-1
反应条件
potassium carbonate in acetone 12 h; Heating;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-84-4
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-85-5
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating 3: pyridine 4: 180 mg / bromine / acetic acid / 2 h View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-86-6
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating 3: 50 mg / 10percent KOH / ethanol / 8 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-87-7
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating 3: 1. OsO4/potassium periodate 2. polyphosphoric acid / 1. water/6 h 2. 2 h/115 deg C View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-88-8
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating 3: 120 mg / konz. H2SO4 / 0.25 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-90-2
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating 3: pyridine View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
108-24-7
乙酸酐
+
88498-80-0
→
反应条件
88498-91-3
反应条件
pyridine
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
