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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88498-84-4
合成路线
（共 8 条）
3722-51-8
西伯尔链接剂
→
反应条件
88498-84-4
反应条件
1: 1.8 g / pyridine hydrobromide perbromide / acetic acid / 0.5 h / 55 °C 2: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 3: 400 mg / decahydronaphthalene / 3 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-80-0
→
反应条件
88498-84-4
反应条件
1: 5 g / anhydrous potassium carbonate / acetone / 12 h / Heating 2: 400 mg / decahydronaphthalene / 3 h / Heating View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-81-1
→
反应条件
731-66-8
+
88498-84-4
反应条件
in decalin 3 h; Heating;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-84-4
→
反应条件
88498-85-5
反应条件
1: pyridine 2: 180 mg / bromine / acetic acid / 2 h View Scheme
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-84-4
→
反应条件
88498-86-6
反应条件
potassium hydroxide in ethanol 8 h; Heating;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-84-4
→
反应条件
88498-87-7
反应条件
osmium(VIII) oxide; potassium meta-periodate 1. water/6 h 2. 2 h/115 deg C; Yield given. Multistep reaction;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
88498-84-4
→
反应条件
88498-88-8
反应条件
sulfuric acid 0.25 h; Heating;
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
108-24-7
乙酸酐
+
88498-84-4
→
反应条件
88498-90-2
反应条件
pyridine
参考文献
Patel, G. N.; Trivedi, K. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 8 p. 755 - 758
