trichlorophosphate in acetonitrile 2 h; Heating;

1: 84 percent / POCl3 / acetonitrile / 2 h / Heating 2: 66 percent / H2 / 10percent Pd/C / methanol / 1 h / 2585.7 Torr View Scheme

&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '1730800', constants.ctx, '0')">dichloromethane</a> <br />0.5&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 98 percent / SOCl₂ / 1.5 h / Heating<br />2: 75 percent / CH₂Cl₂ / 0.5 h<br /> <br /> &nbsp;