5,11-二氢-6H-吡啶并[2,3-B][1,4]苯并二氮杂-6-酮合成路线 （共 23 条）
反应条件
1: 95 percent / 40percent H2O2, acetic acid / 50 deg C, 3 h, then 20-25 deg C, 24 h
2: acetonitrile / 2 h / 80 °C
3: 100 percent / toluene / 2 h / 80 °C
4: H2 / Raney nickel / ethanol / 8 h / 60 °C
View Scheme
参考文献
Kovac, T.; Oklobdzija, M.; Comisso, G.; Decorte, E.; Fajdiga, T.; et al.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1339 - 1349
反应条件
1: 95 percent / 40percent H2O2, acetic acid / 50 deg C, 3 h, then 20-25 deg C, 24 h
2: acetonitrile / 2 h / 80 °C
3: 100 percent / toluene / 2 h / 80 °C
View Scheme
参考文献
Kovac, T.; Oklobdzija, M.; Comisso, G.; Decorte, E.; Fajdiga, T.; et al.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1339 - 1349
反应条件
1: 95 percent / 40percent H2O2, acetic acid / 50 deg C, 3 h, then 20-25 deg C, 24 h
2: 65 percent / 50percent aq. KOH / tetrabutylammonium chloride / toluene / 4 h / Heating
View Scheme
参考文献
Kovac, T.; Oklobdzija, M.; Comisso, G.; Decorte, E.; Fajdiga, T.; et al.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1339 - 1349
