4,4-二甲基二苯基甲醇合成路线 （共 56 条）
反应条件
C42H62ClO3PPd; sodium salt of phosphorous acid in toluene T=50°C; 30 h;
参考文献
Liao, Yuan-Xi; Xing, Chun-Hui; Israel, Matthew; Hu, Qiao-Sheng
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3324 - 3328
反应条件
hydrogen in tetrahydrofuran T=60°C; P=760.051 Torr; 45 h;
参考文献
Zhang, Guoqi; Scott, Brian L.; Hanson, Susan K.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 48 p. 12102 - 12106
Angew. Chem., 2012 , p. 12077
反应条件
Rh2(trifluoroacetate)4(1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene)2; potassium tert-butylate in methanol T=65°C; 3 h; Inert atmosphere;
参考文献
Trindade, Alexandre F.; Andre, Vania; Duarte, M. Teresa; Veiros, Luis F.; Gois, Pedro M.P.; Afonso, Carlos A.M.
Tetrahedron, 2010 , vol. 66, # 44 p. 8494 - 8502
反应条件
1: para-bromotoluene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; 2: formic acid ethyl ester in tetrahydrofuran; hexane T=-78°C; 3 h; 3: With ethanol; iodine; potassium carbonate in tetrahydrofuran; hexane T=-78 - 20°C; 14 h;
参考文献
Tetrahedron, , vol. 68, # 24 p. 4701 - 4709
反应条件
magnesium 1.) diethyl ether, 2.) 0.5 h; Yield given. Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 112, # 8 p. 3068 - 3082
反应条件
hydrogen fluoride; boron trifluoride T=45°C; P=37503.8 - 60006 Torr; 1 h; Further byproducts.;
参考文献
Synthesis, , # 15 p. 2543 - 2550
反应条件
1: para-bromotoluene With magnesium in tetrahydrofuran 1 h; Inert atmosphere; 2: 4-chlorobenzaldehyde in tetrahydrofuran T=20°C; 2 h; Inert atmosphere;
参考文献
Mori, Keiji; Sueoka, Shosaku; Akiyama, Takahiko
Chemistry Letters, 2009 , vol. 38, # 6 p. 628 - 629
反应条件
aluminium; sodium chloride in ammonia T=25°C; 4 h; Irradiation;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 63, # 1 p. 290 - 292
反应条件
water in acetone T=25°C; Kinetics; Further Variations:Solvents;
参考文献
Angewandte Chemie - International Edition, , vol. 43, # 17 p. 2302 - 2305
反应条件
potassium phosphate; platinacycle in toluene T=90 - 100°C; 2 h;
参考文献
Liao, Yuan-Xi; Hu, Qiao-Sheng
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6986 - 6989
