4,4-二甲基二苯基甲醇合成路线 （共 56 条）
反应条件
1: iodine / dichloromethane / 0.75 h / 25 °C 2: iodine / neat (no solvent) / 0.6 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
tert.-butylhydroperoxide; bismuth(III)oxide in water; ethyl acetate 4 h; Reflux; Kinetics; Concentration; chemoselective reaction;
参考文献
Malik, Payal; Chakraborty, Debashis
Synthesis, 2010 , # 21 art. no. Z17610SS, p. 3736 - 3740
反应条件
in water T=435°C; 1.5 h; supercritical;
参考文献
Tetrahedron Letters, , vol. 43, # 33 p. 5859 - 5861
反应条件
tris(triphenylphosphine)ruthenium(II) chloride in various solvent(s) T=180°C; 3 h; Product distributionRate constant;
参考文献
Pri-Bar, Ilan; Buchman, Ouri; Schumann, Hebert; Kroth, Heinz J.; Blum, Jochanan
Journal of Organic Chemistry, 1980 , vol. 45, # 22 p. 4418 - 4428
反应条件
1: iodine / dichloromethane / 0.75 h / 25 °C 2: iodine / neat (no solvent) / 0.6 h / 85 °C 3: iodine / neat (no solvent) / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
1: iodine / dichloromethane / 0.75 h / 25 °C 2: iodine / neat (no solvent) / 0.6 h / 85 °C View Scheme
参考文献
Jereb, Marjan; Vrazic, Dejan
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 12 p. 1978 - 1999
反应条件
hydrogenchloride; calcium chloride in dichloromethane
参考文献
Auricchio, Sergio; Magnani, Caterina; Truscello, Ada M.
European Journal of Organic Chemistry, 2002 , # 14 p. 2411 - 2416
反应条件
diethyl ether
anschliessend Erwaermen mit Oxalsaeure-diaethylester;
参考文献
Lapkin; Lapkina
Zhurnal Obshchei Khimii, 1955 , vol. 25, p. 298,301; engl. Ausg. S. 281, 283
反应条件
T=60°C; Equilibrium constant;
参考文献
Halford; Reid
Journal of the American Chemical Society, 1941 , vol. 63, p. 1873,1876
反应条件
thionyl chloride in benzene
1 h; Heating;
参考文献
Dutta; Xu; Reith
Journal of Medicinal Chemistry, 1996 , vol. 39, # 3 p. 749 - 756
