Seo, Seon-M.I.; Junheon, Kim; Eunae, Kim; Park, Hye-M.I.; Kim, Young-Joon; Park, I.L.-Kwon
Journal of Agricultural and Food Chemistry, 2010 , vol. 58, # 3 p. 1823 - 1827
1: 2-(2-propynyloxy)-tetrahydro-2H-pyran With n-butyllithium in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=-78°C;
2: 1-bromo-octane in tetrahydrofuran
参考文献
Stefani, Helio A.; Cardoso, Lincoln D. G.; Valduga, Claudete J.; Zeni, Gilson
Phosphorus, Sulfur and Silicon and Related Elements, 2001 , vol. 171-172, p. 167 - 172
1: diethylzinc; (Z)-1-Iodo-non-4-ene With copper(l) iodide
T=60°C; 16 h;
2: 1-tetrahydropyranyloxy-9-iodo-2-nonyne With N,N'-dimethyl-N,N'-propyleneurea; Me2Cu(CN)(MgCl)2 in tetrahydrofuran
T=-78 - 0°C; Further stages. Title compound not separated from byproducts.;
