2-甲酰基-4-甲基苯氧基乙酸合成路线 （共 7 条）
反应条件
sodium acetate; acetic anhydride T=110°C; 3 h;
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
1: 81.6 percent / K2CO3 / tetrahydrofuran / 3 h / Heating
2: 83.3 percent / 20percent aq. KOH / ethanol / 0.5 h / 60 °C
View Scheme
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
potassium hydroxide in methanol
参考文献
Hullar,T.L.; Failla,D.L.
Journal of Medicinal Chemistry, 1969 , vol. 12, # 3 p. 420 - 424
反应条件
sodium ethanolate
entsteht der Aethylester;
参考文献
v. Auwers
Justus Liebigs Annalen der Chemie, 1912 , vol. 393, p. 358
Justus Liebigs Annalen der Chemie, 1915 , vol. 408, p. 280
参考文献
Hoechster Farbw.
Patent: DE362382 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 14, p. 1160
反应条件
sodium acetate; acetic anhydride
T=110°C; 3 h;
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
反应条件
1: 55.5 percent / AcONa, Ac2O / 3 h / 110 °C
2: 87.5 percent / diethyl ether / 0.33 h / Ambient temperature
View Scheme
参考文献
Suzuki; Horaguchi; Shimizu; Abe
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 9 p. 2762 - 2767
