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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
1-CBZ-4-碘哌啶
合成路线
（共 7 条）
885275-00-3
1-CBZ-4-碘哌啶
→
反应条件
66207-23-6
N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶
+
3742-91-4
1-哌啶羧酸苄酯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Chemical Communications, , vol. 50, # 28 p. 3725 - 3728
292638-84-7
+
885275-00-3
1-CBZ-4-碘哌啶
→
反应条件
66207-23-6
N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶
+
3742-91-4
1-哌啶羧酸苄酯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Chemical Communications, , vol. 50, # 28 p. 3725 - 3728
292638-84-7
+
885275-00-3
1-CBZ-4-碘哌啶
→
反应条件
66207-23-6
N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Zou, Yinjun; Zhou, Jianrong
Chemical Communications, 2014 , vol. 50, # 28 p. 3725 - 3728
95798-23-5
1-Cbz-4-羟基哌啶
→
反应条件
885275-00-3
1-CBZ-4-碘哌啶
反应条件
1H-imidazole; iodine; triphenylphosphine in dichloromethane Inert atmosphereDarkness;
参考文献
Smith, Sean W.; Fu, Gregory C.
Angewandte Chemie - International Edition, 2008 , vol. 47, # 48 p. 9334 - 9336
885275-00-3
1-CBZ-4-碘哌啶
→
反应条件
66207-23-6
N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶
+
3742-91-4
1-哌啶羧酸苄酯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Zou, Yinjun; Zhou, Jianrong
Chemical Communications, 2014 , vol. 50, # 28 p. 3725 - 3728
292638-84-7
+
885275-00-3
1-CBZ-4-碘哌啶
→
反应条件
66207-23-6
N-苯甲氧基甲酰基-1,2,5,6-四氢吡啶
+
3742-91-4
1-哌啶羧酸苄酯
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tetrakis(triphenylphosphine) palladium(0); cyclohexa-1,4-diene; α,α,α-trifluorotoluene; N,N-dicyclohexylmethylamine T=110°C; Heck Reaction; 12 h; Inert atmosphereGlovebox; Mechanism;
参考文献
Zou, Yinjun; Zhou, Jianrong
Chemical Communications, 2014 , vol. 50, # 28 p. 3725 - 3728
885275-00-3
1-CBZ-4-碘哌啶
+
93-97-0
苯甲酸酐
→
反应条件
922504-27-6
反应条件
bis(1,5-cyclooctadiene)nickel (0); bathophenanthroline; magnesium chloride; zinc in acetonitrile T=25°C; 12 h; Inert atmosphere;
参考文献
Yin, Hongyu; Zhao, Chenglong; You, Hengzhi; Lin, Kunhua; Gong, Hegui
Chemical Communications, 2012 , vol. 48, # 56 p. 7034 - 7036
