4-溴-1-(溴甲基)-2-碘苯合成路线 （共 2 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in 1,2-dichloro-ethane
5 h; Inert atmosphereRefluxIrradiation;
参考文献
THE JOHNS HOPKINS UNIVERSITY; TOVAR, John Dayton; CARUSO, Jr., Anthony
Patent: WO2011/127383 A2, 2011 ;
Location in patent: Page/Page column 74 ;
反应条件
1: sodium periodate; sulfuric acid; iodine; acetic anhydride; acetic acid / 0 - 20 °C / Inert atmosphere
2: N-bromosuccinmide; dibenzoyl peroxide / 1,2-dichloro-ethane / 5 h / Inert atmosphere; Reflux; Irradiation
View Scheme
参考文献
Caruso, Anthony; Tovar, John D.
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2227 - 2239
