反应条件
1: trichlorophosphate; N-ethyl-N,N-diisopropylamine / 1,4-dioxane / 7 h / 100 °C / |Large scale 2: chloro-difluoro-acetic acid methyl ester; potassium fluoride; copper(II) bis(trifluoromethanesulfonate) / N,N-dimethyl acetamide / 120 °C View Scheme
参考文献
Mulder, Jason A.; Frutos, Rogelio P.; Patel, Nitinchandra D.; Qu, Bo; Sun, Xiufeng; Tampone, Thomas G.; Gao, Joe; Sarvestani, Max; Eriksson, Magnus C.; Haddad, Nizar; Shen, Sherry; Song, Jinhua J.; Senanayake, Chris H.
Organic Process Research and Development, 2013 , vol. 17, # 6 p. 940 - 945