反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
1: 70 percent / Cp2ZrEt2 / tetrahydrofuran / 1 h / -78 - 20 °C 2: CuCl; water / tetrahydrofuran / 12 h / 50 °C 3: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 52 p. 12842 - 12848
反应条件
1: 75 percent / CuCl; water / tetrahydrofuran / 3 h / 50 °C 2: 77 percent / conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 52 p. 12842 - 12848
反应条件
1: CuCl; water / tetrahydrofuran / 12 h / 50 °C 2: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 52 p. 12842 - 12848
反应条件
1: CuCl; water / tetrahydrofuran / 12 h / 50 °C 2: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 52 p. 12842 - 12848
反应条件
1: 67 percent / Cp2ZrEt2 / tetrahydrofuran / 1 h / -78 - 20 °C 2: CuCl; water / tetrahydrofuran / 12 h / 50 °C 3: conc. HCl / tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 119, # 52 p. 12842 - 12848
反应条件
1: electrolysis 2: TCA / acetonitrile / 0 °C / Irradiation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, # 17 p. 5270 - 5271
反应条件
n-butyllithium; trifuran-2-yl-phosphane; nickel dichloride in tetrahydrofuran; hexane T=60°C; 4 h; Inert atmosphere;
参考文献
Synlett, , # 13 p. 2061 - 2063
反应条件
NiCl2(dppe) in tetrahydrofuran T=60°C; 4 h; Inert atmosphere;
参考文献
Synlett, , # 13 p. 2061 - 2063
反应条件
triethylsilane; 1,1'-bis-(diphenylphosphino)ferrocene; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; water; copper(II) sulfate in toluene 24 h; Reflux; stereoselective reaction;
参考文献
Luo, Fang; Pan, Changduo; Wang, Wenhui; Ye, Zhishi; Cheng, Jiang
Tetrahedron, 2010 , vol. 66, # 6 p. 1399 - 1403
反应条件
anhydrous lithium acetate; palladium diacetate; triphenylphosphine; lithium chloride in N,N-dimethyl-formamide T=120°C; Inert atmosphere;
参考文献
Yamashita, Mana; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 4 p. 631 - 636