反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
1.1: 94 percent / tetrahydrofuran / 12 h / 20 °C 2.1: NaHMDS / tetrahydrofuran / 8 h / 20 °C 2.2: 94 percent / tetrahydrofuran / 0.25 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 10 p. 3521 - 3524
参考文献
Journal of the American Chemical Society, , vol. 60, p. 2333,2335
反应条件
NiCl2((PPh3)P)2 in benzene 8 h; Heating;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 9 p. 617 - 618
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; diethyl ether T=20°C; 0.5 h;
参考文献
Bumagin, N. A.; Kasatkin, A. N.; Beletskaya, I. P.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1984 , vol. 33, p. 1696 - 1703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1984 , # 8 p. 1858 - 1865
反应条件
lt;CoH(N2)(PPh3)3gt; in acetonitrile T=22°C; 23 h; Title compound not separated from byproducts;
参考文献
Monatshefte fuer Chemie, , vol. 119, p. 583 - 590
反应条件
[(PPh3)3Pd]; triphenylphosphine in N,N-dimethyl-formamide T=80°C; 3 h; Yield given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 59, # 4 p. 1279 - 1280
反应条件
tetrakis(triphenylphosphine) palladium(0) in acetonitrile T=25°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 526, # 2 p. 335 - 339
反应条件
palladium diacetate; triethylamine in acetonitrile T=25°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 526, # 2 p. 335 - 339
反应条件
palladium diacetate; triethylamine in acetonitrile T=82°C; 2 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 526, # 2 p. 335 - 339
反应条件
dilithium tetrachloropalladate; silver(I) acetate in acetonitrile T=25°C; 20 h; Yield given. Yields of byproduct given;
参考文献
Journal of Organometallic Chemistry, , vol. 526, # 2 p. 335 - 339