反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
Lawesson's reagent in toluene 0.5 h; Heating;
参考文献
Nishio, Takehiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1113 - 1118
反应条件
HZSM-5 zeolite in 2,2,4-trimethylpentane T=20°C; 2 h; Irradiation; Product distribution; Further Variations:ReagentsSolventsother substrates;
参考文献
Journal of the American Chemical Society, , vol. 127, # 41 p. 14497 - 14504
反应条件
in deuterated toluene Title compound not separated from byproducts.;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 48 p. 8180 - 8184
反应条件
1: 100 percent / Pd(OAc)2 / diethyl ether / 10 h / 0 °C 2: 95 percent / NaBH4 / methanol / 2 h / 0 °C 3: 95 percent / In(OTf)3 / CH2Cl2 / 0.42 h / ultrasound View Scheme
参考文献
European Journal of Organic Chemistry, , # 13 p. 3012 - 3015
反应条件
KF*2H2O; Pd(quinox)Cl2 in isopropyl alcohol T=20°C; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 134, # 28 p. 11408 - 11411
反应条件
1: With n-butyllithium; zirconocene dichloride in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphereSchlenk technique; 2: With hydrogenchloride; water in tetrahydrofuran; hexane Inert atmosphereSchlenk technique;
参考文献
Chemistry Letters, , vol. 40, # 12 p. 1443 - 1444
反应条件
N,N'-diphenyl-1,4-benzoquinone-1,4-diimine in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; Overall yield = 99 percentSpectr.;
参考文献
Chemistry - A European Journal, , vol. 20, # 3 p. 653 - 656
反应条件
benzenesulfonamide monosodium salt in chlorobenzene 1 h; Heating;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 6.2 p. 1159 - 1162
Zhurnal Organicheskoi Khimii, , vol. 25, # 6 p. 1288 - 1292
反应条件
sodium hydroxide in dichloromethane 2 h; Ambient temperature;
参考文献
Clarke, Stephen D.; Harrison, Charles R.; Hodge, Philip
Tetrahedron Letters, 1980 , vol. 21, p. 1375 - 1378
反应条件
1: 67 percent / chlorobenzene / 2 h / Heating 2: 51 percent / sodiobenzenesulfonamide / chlorobenzene / 1 h / Heating View Scheme
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 25, # 6.2 p. 1159 - 1162
Zhurnal Organicheskoi Khimii, , vol. 25, # 6 p. 1288 - 1292