反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
1-methyl-pyrrolidin-2-one; copper(l) iodide; sodium chloride T=120°C; 12 h; other reagent: MnBr2, NaCl, N-methylpyrrolidone;
参考文献
Kang, Suk-Ku; Kim, Jae-Sun; Choi, Sang-Chul
Journal of Organic Chemistry, 1997 , vol. 62, # 13 p. 4208 - 4209
反应条件
[14C]-Orotic acid; caesium carbonate in acetone T=80°C; Suzuki coupling; 30 h; Inert atmosphere;
参考文献
Zhang, Hong-Ping; Dai, You-Zhi; Zhou, Xi; Yu, Huang
Synlett, 2012 , vol. 23, # 8 p. 1221 - 1224
反应条件
chloro-trimethyl-silane; bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran T=20°C; 8 h;
参考文献
Wang, Jin-Xian; Wang, Kehu; Zhao, Lianbiao; Li, Hongxia; Fu, Ying; Hu, Yulai
Advanced Synthesis and Catalysis, 2006 , vol. 348, # 10-11 p. 1262 - 1270
反应条件
[2,2']bipyridinyl; NiBr2bipy in various solvent(s) T=20°C; electrochemical reaction, magnesium anode, gold gauze cathode, -1,2 V;
参考文献
Rollin, Yolande; Troupel, Michel; Tuck, Dennis G.; Perichon, Jacques
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 131 - 138
反应条件
1: N'-[benz-(E)-ylidene]-p-toluenesulfonohydrazide With potassium tert-butylate in toluene T=0 - 20°C; 1 h; 2: (E)-cinnamaldehyde With 5,10,15,20-tetraphenyl porphyrinato iron hydroxide; Aliquatreg; 336; phosphorous acid trimethyl ester in toluene T=40°C; Wittig olefination; 48 h;
参考文献
Journal of the American Chemical Society, , vol. 125, # 20 p. 6034 - 6035
反应条件
carbon dioxide; aluminium; 1-n-butyl-3-methylimidazolium bistrifluoromethylsulfonylamide T=45°C; Ullmann reaction; P=116262 Torr; 12 h;
参考文献
Cheng, Jinsheng; Zhang, Gencheng; Du, Jin; Tang, Longhua; Xu, Jingying; Li, Jinghong
Journal of Materials Chemistry, 2011 , vol. 21, # 10 p. 3485 - 3494
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Walborsky, H. M.; Wuest, H. H.
Journal of the American Chemical Society, 1982 , vol. 104, # 21 p. 5807 - 5808
反应条件
silver(l) oxide; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; water T=20°C; Suzuki-Miyaura cross-coupling reaction; 12 h;
参考文献
Babudri, Francesco; Farinola, Gianluca M.; Naso, Francesco; Ragni, Roberta; Spina, Giulia
Synthesis, 2007 , # 19 p. 3088 - 3092
反应条件
potassium carbonate; bis(η3-allyl-μ-chloropalladium(II)) in N,N-dimethyl-formamide T=130°C; Heck reaction; 20 h;
参考文献
Lemhadri, Mhamed; Battace, Ahmed; Berthiol, Florian; Zair, Touriya; Doucet, Henri; Santelli, Maurice
Synthesis, 2008 , # 7 p. 1142 - 1152
反应条件
dichloro bis(acetonitrile) palladium(II) in N,N-dimethyl-formamide T=25°C; 0.1 h;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 813