反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
T=250°C; Diels-Alder Cycloaddition; 24 h;
参考文献
Tetrahedron Letters, , vol. 54, # 15 p. 1991 - 1993
反应条件
1: sodium acetate; xylene / Erhitzen des Reaktionsprodukts mit Schwefel auf 200grad 2: NaNH2; cymene View Scheme
参考文献
Journal of the American Chemical Society, , vol. 62, p. 656,660
反应条件
isopropylmagnesium chloride in diethyl ether; argon
反应条件
9,10-anthracenedicarbonitrile; oxygen in acetonitrile Oxidation; Irradiation; Product distribution; Further Variations:Solvents;
参考文献
Li, Hong Ru; Wu, Li Zhu; Tung, Chen Ho
Chemical Communications, 2000 , # 12 p. 1085 - 1086
反应条件
9,10-anthracenedicarbonitrile; oxygen in various solvent(s) Oxidation; Irradiation; Product distribution; Further Variations:ReagentsSolvents;
参考文献
Li, Hong-Ru; Wu, Li-Zhu; Tung, Chen-Ho
Tetrahedron, 2000 , vol. 56, # 38 p. 7437 - 7442
反应条件
in dichloromethane 72 h; Irradiation; Mechanism;
参考文献
Chemische Berichte, , vol. 114, # 8 p. 2844 - 2858
反应条件
1: 75 percent / O2, tetraphenylporphine (TPP) / CCl4 / 2 h / 15 °C / Irradiation 2: 36 percent / tetracyanoethylene (TCNE) / CH2Cl2 / 4 h / Irradiation; other endoperoxides; var. time of irradiation View Scheme
参考文献
Suzuki, Masaaki; Ohtake, Hiroaki; Kameya, Yoshimi; Hamanaka, Nobuyuki; Noyori, Ryoji
Journal of Organic Chemistry, 1989 , vol. 54, # 22 p. 5292 - 5302
反应条件
in hexane Os-cluster and ligand were placed in tube with hexane, heated for 15 h at 85°C under N2; solvent and volatiles were removed in vacuo, TLC with hexane-CH2Cl2;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 6 p. 1020 - 1023
反应条件
in hexane Os-cluster and ligand were placed in tube with hexane, heated for 15 h at 85°C under N2; solvent and volatiles were removed in vacuo, TLC with hexane-CH2Cl2; elem. anal.;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 6 p. 1020 - 1023
反应条件
hydrogenchloride; peroxynitrous acid in water; acetonitrile T=5 - 10°C; pH=0; 1 h; Further byproducts given;
参考文献
European Journal of Organic Chemistry, , # 4 p. 741 - 748