反,反-1,4-二苯基-1,3-丁二烯合成路线 (共 318 条)
反应条件
1: 215 °C 2: 168 h / 230 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 103, # 15 p. 4595 - 4597
反应条件
2: ethanolic KOH View Scheme
参考文献
Alder; Niklas
Justus Liebigs Annalen der Chemie, 1954 , vol. 585, p. 81,92
反应条件
Fe(CO)3*PhCH=CH(Me)CHO in toluene T=70°C; Rate constant;
参考文献
Burkinshaw, Philip M.; Dixon, Denis T.; Howell, James A. S.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1980 , p. 999 - 1004
反应条件
1: benzene 2: methanol; benzene 3: aq. acid View Scheme
参考文献
Halton,B. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 731 - 735
反应条件
1: benzene 2: KOtBu / tetrahydrofuran View Scheme
参考文献
Halton,B. et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1977 , p. 731 - 735
反应条件
magnesium THF; 1.) room temp., 2 h; 2.) -78 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rieke, Reuben D.; Xiong, Heping
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 3109 - 3118
反应条件
magnesium THF; 1.) room temp., 2 h; 2.) -78 deg C, 2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Rieke, Reuben D.; Xiong, Heping
Journal of Organic Chemistry, 1991 , vol. 56, # 9 p. 3109 - 3118
反应条件
1: 80 percent / xylene / 15 h / 137 - 144 °C 2: 87 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / toluene / 18 h / 111 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 72, # 8 p. 3020 - 3030
反应条件
nitrobenzene T=200°C;
参考文献
Lukas, B.; Roberts, R. M. G.; Silver, J.; Wells, A. S.
Journal of Organometallic Chemistry, 1983 , vol. 256, # 1 p. 103 - 110