反,反-1,4-二苯基-1,3-丁二烯合成路线 （共 318 条）
反应条件
1: With lithium vanadium(I) dihydride in tetrahydrofuran
T=25°C; 12 h; Inert atmosphere;
2: With hydrogenchloride in water
参考文献
Eisch, John J.; Fregene, Paul O.
European Journal of Organic Chemistry, 2008 , # 26 p. 4482 - 4492
参考文献
Diels; Alder
Justus Liebigs Annalen der Chemie, 1926 , vol. 450, p. 245
反应条件
1: methylcyclohexane; Raney nickel / 45 °C / 29420.3 - 47808 Torr / Hydrogenation
3: xylene; sodium
View Scheme
参考文献
Cram; Steinberg
Journal of the American Chemical Society, 1951 , vol. 73, p. 5691,5698
反应条件
zeolite Ca Y in hexane
T=22°C; 0.0833333 h;
参考文献
Pitchumani; Joy, Abraham; Prevost, Nicolette; Ramamurthy
Chemical Communications, 1997 , # 1 p. 127 - 128
反应条件
1: propan-2-ol
2: Br2 / CHCl3
View Scheme
参考文献
Ried,W.; Boennighausen,K.H.
Justus Liebigs Annalen der Chemie, 1961 , vol. 639, p. 61 - 67
反应条件
1: 214 - 217 °C
2: Se
3: benzene / 4 h / Heating
4: 50 percent / Irradiation
View Scheme
参考文献
Tomioka, Hideo; Miura, Shinichi; Izawa, Yasuji
Tetrahedron Letters, 1983 , vol. 24, # 32 p. 3353 - 3356
反应条件
in 1,2-dichloro-ethane
T=65 - 75°C; 3 h;
参考文献
Chen, Zhengbo; Shou, Wangge; Wang, Yanguang
Synthesis, 2009 , # 7 art. no. F21708SS, p. 1075 - 1080
反应条件
1: 1.) NBS / 1.) CH2Cl2, 2 min, 2.) CH2Cl2, 5 h
2: 68 percent / NBS, benzoyl peroxide / CCl4 / 2 h / Heating; Irradiation
3: 0.67 h / 110 °C / 1 Torr
View Scheme
参考文献
Sheradsky, Tuvia; Moshenberg, Reuven
Journal of Organic Chemistry, 1986 , vol. 51, # 16 p. 3123 - 3125
反应条件
in acetonitrile
T=0°C; 12 h;
参考文献
Bronberger, Franz; Huisgen, Rolf
Tetrahedron Letters, 1984 , vol. 25, # 1 p. 57 - 60
反应条件
lithium biphenylide; CaI2
1.) THF, room temperature, 2.) -78 to -60 deg C; Yield given. Multistep reaction;
参考文献
Sell; Rieke
Synthetic Communications, 1995 , vol. 25, # 24 p. 4107 - 4113
