2-(N-丙基氨基甲酰)-1,2,3,4-四氢异喹啉合成路线 （共 7 条）
反应条件
in dichloromethane
T=20°C; 12 h;
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 88 percent / pyridine / CH2Cl2 / 2 h / 20 °C
2: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 62 percent / LiAlH4 / tetrahydrofuran / Heating
2: 100 percent Spectr. / tetrahydrofuran / 1 h / 20 °C
3: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 2.48 g / LiAlH4 / tetrahydrofuran / 36 h / Heating
2: 3 percent Spectr. / diethyl ether / 1 h / 20 °C
3: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 3 percent Spectr. / diethyl ether / 1 h / 20 °C
2: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 100 percent Spectr. / tetrahydrofuran / 1 h / 20 °C
2: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
反应条件
1: 100 percent Spectr. / CH2Cl2 / 0.5 h / 20 °C
2: 95 percent / CH2Cl2 / 12 h / 20 °C
View Scheme
参考文献
Lemoucheux, Laurent; Rouden, Jacques; Ibazizene, Meziane; Sobrio, Franck; Lasne, Marie-Claire
Journal of Organic Chemistry, 2003 , vol. 68, # 19 p. 7289 - 7297
