反应条件
1: 2,6-Dibromopyridine With n-butyllithium in tetrahydrofuran; diethyl ether; hexane
T=-95 - -90°C; Inert atmosphere;
2: trifluoro acetic acid methyl ester in tetrahydrofuran; diethyl ether; hexane
T=-100 - -90°C; 0.5 h; Inert atmosphere;
参考文献
Zhu, Di; Janssen, Femke F. B. J.; Budzelaar, Peter H. M.
Organometallics, 2010 , vol. 29, # 8 p. 1897 - 1908