5-氯-3-甲基吡啶-2-羧酸合成路线 （共 2 条）
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; triethylamine; palladium diacetate in methanol T=100°C; P=2585.81 Torr; 11 h;
参考文献
Albaneze-Walker, Jennifer; Ceglia, Scott; Murry, Jerry Anthony; Soheili, Arash
Patent: US2004/102472 A1, 2004 ;
Location in patent: Page 49; 50 ;
US 20040102472 A1
反应条件
1: in tetrahydrofuran
T=5 - 30°C;
2: With hydrogenchloride in tetrahydrofuran; methanol; water; ethyl acetate
T=30°C; pH=4;
3: With sodium hydroxide in water
pH=8;
参考文献
Albaneze-Walker, Jennifer; Ceglia, Scott; Murry, Jerry Anthony; Soheili, Arash
Patent: US2004/102472 A1, 2004 ;
Location in patent: Page 50 ;
US 20040102472 A1
