10-氧代-4,9-二氮杂螺[4.5]癸烷-4-羧酸叔丁酯合成路线 （共 3 条）
反应条件
1.1: 74 percent / DMAP; Et3N / CH2Cl2 / 20 °C
2.1: LiHMDS / tetrahydrofuran
2.2: potassium carbonate / methanol
3.1: toluene / Heating
View Scheme
参考文献
Kelleher, Fintan; Kelly, Sinead
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3005 - 3008
反应条件
1.1: LiHMDS / tetrahydrofuran
1.2: potassium carbonate / methanol
2.1: toluene / Heating
View Scheme
参考文献
Kelleher, Fintan; Kelly, Sinead
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3005 - 3008
反应条件
1.1: 94 percent / SOCl2 / Heating
2.1: 74 percent / DMAP; Et3N / CH2Cl2 / 20 °C
3.1: LiHMDS / tetrahydrofuran
3.2: potassium carbonate / methanol
4.1: toluene / Heating
View Scheme
参考文献
Kelleher, Fintan; Kelly, Sinead
Tetrahedron Letters, 2006 , vol. 47, # 18 p. 3005 - 3008
