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乙二醇
甲醛
63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
88704-48-7
合成路线
（共 16 条）
126893-01-4
→
反应条件
88704-48-7
反应条件
boron tribromide in dichloromethane 5 h; Heating;
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
77549-09-8
→
反应条件
88704-48-7
反应条件
1: 1.) H3PO4 / 1.) RT, 17 min, 2.) pyridine, RT 2: 88 percent / K2CO3 / methanol; acetone / 12 h / Ambient temperature 3: 60 percent / K2CO3 / acetone / 48 h / Heating 4: 79 percent / NBS / acetic acid; dioxane / 1 h / Ambient temperature 5: 84 percent / KOH / ethanol; H2O / 4 h / Heating 6: 89 percent / DCC, Et3N / CH2Cl2 7: 84 percent / PPE / 1,2-dichloro-ethane 8: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 9: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-11-6
→
反应条件
88704-48-7
反应条件
1: 60 percent / K2CO3 / acetone / 48 h / Heating 2: 79 percent / NBS / acetic acid; dioxane / 1 h / Ambient temperature 3: 84 percent / KOH / ethanol; H2O / 4 h / Heating 4: 89 percent / DCC, Et3N / CH2Cl2 5: 84 percent / PPE / 1,2-dichloro-ethane 6: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 7: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-12-7
→
反应条件
88704-48-7
反应条件
1: 79 percent / NBS / acetic acid; dioxane / 1 h / Ambient temperature 2: 84 percent / KOH / ethanol; H2O / 4 h / Heating 3: 89 percent / DCC, Et3N / CH2Cl2 4: 84 percent / PPE / 1,2-dichloro-ethane 5: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 6: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-13-8
→
反应条件
88704-48-7
反应条件
1: 62 percent / KOH / ethanol; H2O / 4 h / Heating 2: 89 percent / DCC, Et3N / CH2Cl2 3: 84 percent / PPE / 1,2-dichloro-ethane 4: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 5: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-10-5
→
反应条件
88704-48-7
反应条件
1: 88 percent / K2CO3 / methanol; acetone / 12 h / Ambient temperature 2: 60 percent / K2CO3 / acetone / 48 h / Heating 3: 79 percent / NBS / acetic acid; dioxane / 1 h / Ambient temperature 4: 84 percent / KOH / ethanol; H2O / 4 h / Heating 5: 89 percent / DCC, Et3N / CH2Cl2 6: 84 percent / PPE / 1,2-dichloro-ethane 7: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 8: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-14-9
→
反应条件
88704-48-7
反应条件
1: 84 percent / KOH / ethanol; H2O / 4 h / Heating 2: 89 percent / DCC, Et3N / CH2Cl2 3: 84 percent / PPE / 1,2-dichloro-ethane 4: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 5: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-07-0
→
反应条件
88704-48-7
反应条件
1: 89 percent / DCC, Et3N / CH2Cl2 2: 84 percent / PPE / 1,2-dichloro-ethane 3: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 4: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
126893-15-0
→
反应条件
88704-48-7
反应条件
1: 78 percent / KOH / ethanol; H2O / 4 h / Heating 2: 89 percent / DCC, Et3N / CH2Cl2 3: 84 percent / PPE / 1,2-dichloro-ethane 4: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 5: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
15761-39-4
BOC-L-脯氨酸
→
反应条件
88704-48-7
反应条件
1: 89 percent / DCC, Et3N / CH2Cl2 2: 84 percent / PPE / 1,2-dichloro-ethane 3: 71 percent / NBS / CH2Cl2 / 0.5 h / Ambient temperature 4: 64 percent / BBr3 / CH2Cl2 / 5 h / Heating View Scheme
参考文献
Hino, Tohru; Lai, Ziping; Seki, Hiroko; Hara, Ritsuko; Kuramochi, Tadao; Nakagawa, Masako
Chemical and Pharmaceutical Bulletin, 1989 , vol. 37, # 10 p. 2596 - 2600
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