1-三氟甲基-1,2-苯碘酰-3(H)-酮合成路线 （共 52 条）
反应条件
cesium fluoride in acetonitrile T=20°C; 22 h;
参考文献
Stanek, Kyrill; Koller, Raffael; Togni, Antonio
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7678 - 7685
反应条件
cesium fluoride in acetonitrile T=20°C; 15 h;
参考文献
Eisenberger, Patrick; Gischig, Sebastian; Togni, Antonio
Chemistry - A European Journal, 2006 , vol. 12, # 9 p. 2579 - 2586
反应条件
1: sodium periodate; acetic acid / water / 4 h / 110 °C 2: 0.25 h / 135 °C 3: cesium fluoride / acetonitrile / 24 h / 20 °C / Inert atmosphere View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 39 p. 9120 - 9123
Angewandte Chemie - International Edition, , vol. 51, # 12 p. 2947 - 2950
反应条件
1: 0.25 h / Heating 2: 6.78 g / 0.25 h / Heating 3: 55 percent / CsF / acetonitrile / 15 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 9 p. 2579 - 2586
反应条件
1: 6.78 g / 0.25 h / Heating 2: 55 percent / CsF / acetonitrile / 15 h / 20 °C View Scheme
参考文献
Chemistry - A European Journal, , vol. 12, # 9 p. 2579 - 2586
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Lin, Xiaoxi; Wang, Guimei; Li, Huaifeng; Huang, Yuanyuan; He, Weiming; Ye, Dandan; Huang, Kuo-Wei; Yuan, Yaofeng; Weng, Zhiqiang
Tetrahedron, 2013 , vol. 69, # 12 p. 2628 - 2632
反应条件
anhydrous copper acetate in methanol T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 51, # 45 p. 5947 - 5949
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique; Reagent/catalystSolvent;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
[iridium(III)(2-phenylpyridine)3]; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in N,N-dimethyl-formamide T=20°C; 12 h; Inert atmosphereIrradiationSchlenk technique; Reagent/catalystSolvent;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
