1-三氟甲基-1,2-苯碘酰-3(H)-酮合成路线 (共 52 条)
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; 20 h; Inert atmosphereSchlenk techniqueIrradiation;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; 20 h; Inert atmosphereSchlenk techniqueIrradiation;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
anhydrous copper acetate in methanol T=20°C; 6 h; Inert atmosphere; regioselective reaction;
参考文献
Shimizu, Ryo; Egami, Hiromichi; Nagi, Tatsuya; Chae, Jungha; Hamashima, Yoshitaka; Sodeoka, Mikiko
Tetrahedron Letters, 2010 , vol. 51, # 45 p. 5947 - 5949
反应条件
anhydrous copper acetate in methanol T=20°C; 12 h;
参考文献
Heterocycles, , vol. 86, # 2 p. 979 - 983
反应条件
trimethylsilyl trifluoromethanesulfonate in dichloromethane T=20°C; 0.0833333 h; Schlenk techniqueInert atmosphere;
参考文献
Heterocycles, , vol. 86, # 2 p. 979 - 983
反应条件
copper(l) chloride in tert-butyl alcohol T=30°C; 24 h; Inert atmosphereSealed tube; Catalytic behavior; SolventTemperatureTime; regioselective reaction;
参考文献
Cai, Shangjun; Chen, Chao; Sun, Zelin; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 40 p. 4552 - 4554
反应条件
iron(II) chloride in acetonitrile T=20°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Parsons, Andrew T.; Senecal, Todd D.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2947 - 2950
反应条件
in methanol T=-78°C; 12 h;
参考文献
Caponea, Stefania; Kieltschb, Iris; Floegela, Oliver; Lelaisa, Gerald; Togni, Antonio; Seebach, Dieter
Helvetica Chimica Acta, 2008 , vol. 91, # 11 p. 2035 - 2056
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Organic Letters, , vol. 16, # 6 p. 1768 - 1771