1-三氟甲基-1,2-苯碘酰-3(H)-酮合成路线 （共 52 条）
反应条件
copper(II)gluconate in tetrachloromethane; water T=80°C; 12 h;
参考文献
He, Zhengbiao; Zhang, Rui; Hu, Mingyou; Li, Lingchun; Ni, Chuanfa; Hu, Jinbo
Chemical Science, 2013 , vol. 4, # 9 p. 3478 - 3483
反应条件
toluene-4-sulfonic acid in acetonitrile T=20°C; Kinetics;
参考文献
Santschi, Nico; Sarott, Roman C.; Otth, Elisabeth; Kissner, Reinhard; Togni, Antonio
Beilstein Journal of Organic Chemistry, 2014 , vol. 10, p. 1 - 6
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
1,10-phenanthroline; tetrabutyl ammonium fluoride; cupric trifluoroacetate in dimethyl sulfoxide T=130°C; 8 h; Inert atmosphereSealed tube;
参考文献
Tetrahedron, , vol. 69, # 12 p. 2628 - 2632
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique; Overall yield = 65 percent; regioselective reaction;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
copper(l) iodide in N,N-dimethyl-formamide T=80°C; 23 h; Inert atmosphereSealed tube; regioselective reaction;
参考文献
Fang, Zhongxue; Ning, Yongquan; Mi, Pengbing; Liao, Peiqiu; Bi, Xihe
Organic Letters, 2014 , vol. 16, # 5 p. 1522 - 1525
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique; Overall yield = 52 percent; regioselective reaction;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
1: 2-(benzhydrylidene-amino)-3-mercapto-propionic acid tert-butyl ester With potassium hexamethylsilazane in tetrahydrofuran T=-78°C; 1 h; Inert atmosphere; 2: Togni’s reagent With Zn(NTf2)2 in tetrahydrofuran T=-78°C; 0.5 h; 3: With sulfuric acid in 1,4-dioxane 12 h; Reflux;
参考文献
MEH ASSOCIATES, INC; HEDIGER, Mark, E.
Patent: WO2011/97421 A1, 2011 ;
Location in patent: Page/Page column 27; 28 ;
反应条件
in dichloromethane T=20°C; 22 h;
参考文献
Kieltsch, Iris; Eisenberger, Patrick; Stanek, Kyrill; Togni, Antonio
Chimia, 2008 , vol. 62, # 4 p. 260 - 263
反应条件
in dichloromethane-d2 T=20°C; 24 h;
参考文献
Eisenberger, Patrick; Kieltsch, Iris; Armanino, Nicolas; Togni, Antonio
Chemical Communications, 2008 , # 13 p. 1575 - 1577
