1-三氟甲基-1,2-苯碘酰-3(H)-酮合成路线 （共 52 条）
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique; Overall yield = 52 percent; regioselective reaction;
参考文献
Organic Letters, , vol. 16, # 6 p. 1768 - 1771
反应条件
[iridium(III)(2-phenylpyridine)3] in N,N-dimethyl-formamide T=20°C; Inert atmosphereIrradiationSchlenk technique;
参考文献
Xie, Jin; Yuan, Xiangai; Abdukader, Ablimit; Zhu, Chengjian; Ma, Jing
Organic Letters, 2014 , vol. 16, # 6 p. 1768 - 1771
反应条件
zinc trifluoromethanesulfonate in toluene T=20°C; 48 h;
参考文献
Koller, Raffael; Stanek, Kyrill; Stolz, Daniel; Aardoom, Raphael; Niedermann, Katrin; Togni, Antonio
Angewandte Chemie, International Edition, 2009 , vol. 48, # 24 p. 4332 - 4336
反应条件
in chloroform-d1 T=20°C; 0.5 h;
参考文献
Koller, Raffael; Stanek, Kyrill; Stolz, Daniel; Aardoom, Raphael; Niedermann, Katrin; Togni, Antonio
Angewandte Chemie, International Edition, 2009 , vol. 48, # 24 p. 4332 - 4336
反应条件
iron(II) chloride in acetonitrile T=20°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Parsons, Andrew T.; Senecal, Todd D.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2947 - 2950
反应条件
tris[fac-2-phenylpyridinato-C2,N]iridium(III); sodium acetate in dimethyl sulfoxide T=20°C; Schlenk techniqueIrradiationInert atmosphere;
参考文献
Xu, Pan; Abdukader, Ablimit; Hu, Kaidong; Cheng, Yixiang; Zhu, Chengjian
Chemical Communications, 2014 , vol. 50, # 18 p. 2308 - 2310
反应条件
iron(II) chloride in acetonitrile T=20°C; 24 h; Inert atmosphere; optical yield given as percent destereoselective reaction;
参考文献
Parsons, Andrew T.; Senecal, Todd D.; Buchwald, Stephen L.
Angewandte Chemie - International Edition, 2012 , vol. 51, # 12 p. 2947 - 2950
反应条件
caesium carbonate in water; acetonitrile T=25°C; 24 h; Inert atmosphereSchlenk techniqueSealed tube;
参考文献
Ji, Guojing; Wang, Xi; Zhang, Songnan; Xu, Yan; Ye, Yuxuan; Li, Ming; Zhang, Yan; Wang, Jianbo
Chemical Communications, 2014 , vol. 50, # 33 p. 4361 - 4363
反应条件
18-crown-6 ether in N,N-dimethyl acetamide T=60°C; 24 h;
参考文献
Stanek, Kyrill; Koller, Raffael; Togni, Antonio
Journal of Organic Chemistry, 2008 , vol. 73, # 19 p. 7678 - 7685
反应条件
anhydrous copper acetate in methanol
T=20°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Shimizu, Ryo; Egami, Hiromichi; Nagi, Tatsuya; Chae, Jungha; Hamashima, Yoshitaka; Sodeoka, Mikiko
Tetrahedron Letters, 2010 , vol. 51, # 45 p. 5947 - 5949
