3,3-二甲基-1-(三氟甲基)-1,2-苯并碘氧杂戊环合成路线 (共 71 条)
反应条件
in acetonitrile T=80°C; 96 h; Inert atmosphere;
参考文献
Wiehn, Matthias S.; Vinogradova, Ekaterina V.; Togni, Antonio
Journal of Fluorine Chemistry, 2010 , vol. 131, # 9 p. 951 - 957
反应条件
tris(trimethylsilyl)silyl chloride in acetonitrile T=80°C; 24 h; Inert atmosphere;
参考文献
Wiehn, Matthias S.; Vinogradova, Ekaterina V.; Togni, Antonio
Journal of Fluorine Chemistry, 2010 , vol. 131, # 9 p. 951 - 957
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate in diethylene glycol dimethyl ether T=35°C; 14 h; Inert atmosphere;
参考文献
Liu, Tianfei; Shen, Qilong
Organic Letters, 2011 , vol. 13, # 9 p. 2342 - 2345
参考文献
Kieltsch, Iris; Eisenberger, Patrick; Stanek, Kyrill; Togni, Antonio
Chimia, 2008 , vol. 62, # 4 p. 260 - 263
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate in diethylene glycol dimethyl ether T=35°C; 14 h; Inert atmosphere;
参考文献
Liu, Tianfei; Shen, Qilong
Organic Letters, 2011 , vol. 13, # 9 p. 2342 - 2345
反应条件
[2,2']bipyridinyl; cupric trifluoroacetate in acetonitrile T=20°C; 12 h; Schlenk techniqueInert atmosphereMolecular sieve;
参考文献
Huang, Yuanyuan; Fang, Xin; Lin, Xiaoxi; He, Weiming; Yuan, Yaofeng; Weng, Zhiqiang; Li, Huaifeng; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 48 p. 9949 - 9953,5
反应条件
in methanol T=-78 - 25°C; Inert atmosphere;
参考文献
Helvetica Chimica Acta, , vol. 91, # 11 p. 2035 - 2056
反应条件
[2,2']bipyridinyl; cupric trifluoroacetate in acetonitrile T=20°C; 12 h; Schlenk techniqueInert atmosphereMolecular sieve;
参考文献
Huang, Yuanyuan; Fang, Xin; Lin, Xiaoxi; He, Weiming; Yuan, Yaofeng; Weng, Zhiqiang; Li, Huaifeng; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 48 p. 9949 - 9953,5
反应条件
1,10-phenanthroline; lithium hydroxide hydrate; CuTC in dichloromethane T=45°C; Inert atmosphere;
参考文献
Liu, Tianfei; Shao, Xinxin; Wu, Yaming; Shen, Qilong
Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 540 - 543
反应条件
[2,2']bipyridinyl; cupric trifluoroacetate in acetonitrile T=20°C; 12 h; Schlenk techniqueInert atmosphereMolecular sieve;
参考文献
Huang, Yuanyuan; Fang, Xin; Lin, Xiaoxi; He, Weiming; Yuan, Yaofeng; Weng, Zhiqiang; Li, Huaifeng; Huang, Kuo-Wei
Tetrahedron, 2012 , vol. 68, # 48 p. 9949 - 9953,5